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" ... contamination from sulphur in the gases from source of heat. This may be done by fitting the crucible in a hole in an asbestos board. The heating of the crucible should be gradually done first over a Bunsen burner for a while and then over a blast... "
The Chemical Analysis of Iron: A Complete Account of All the Best Known ... - Seite 217
von Andrew Alexander Blair - 1906 - 318 Seiten
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The Chemical Analysis of Iron: A Complete Account of All the Best Known ...

Andrew Alexander Blair - 1876 - 456 Seiten
...nitrate. Transfer to a large platinum crucible, and fuse well for about an hour at a high temperature. Run the fused mass well up on the sides of the crucible, allow it to cool, dissolve in hot water, and filter. Dilute the filtrate to about 600 cc, and add nitric...
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A Treatise on Chemistry and Chemical Analysis: Quantitative analysis

1899 - 688 Seiten
...combustion to enter the crucible. When the contents of the crucible are in a state of quiet fusion, run the mass well up on the sides of the crucible, and allow it to cool. Dissolve the fusion out of the crucible with hot water, wash the crucible thoroughly, boil the fusion...
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The Chemical and Physical Examination of Portland Cement

Richard Kidder Meade - 1901 - 206 Seiten
...blast-lamp, until the contents of the crucible are in quiet fusion. Remove the crucible from the flame and run the fused mass well up on the sides of the crucible by tilting and revolving the latter while held with the crucible tongs. While still hot plunge the...
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International Library of Technology: A Series of Textbooks for ..., Band 17

1902 - 1004 Seiten
...combustion to enter the crucible. When the contents of the crucible are in a state of quiet fusion, run the mass well up on the sides of the crucible, and allow it to cool. Dissolve the fusion out of the crucible with hot water, wash the crucible thoroughly, boil the fusion...
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Qualitative Analysis: Quantitative Analysis

1902 - 1022 Seiten
...combustion to enter the crucible. When the contents of the crucible are in a state of quiet fusion, run the mass well up on the sides of the crucible, and allow it to cool. Dissolve the fusion out of the crucible with hot water, wash the crucible thoroughly, boil the fusion...
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Portland Cement: Its Composition, Raw Materials, Manufacture, Testing and ...

Richard Kidder Meade - 1906 - 418 Seiten
...burner for a while and then over a blast lamp, until the contents of the crucible are in quiet fusion. Run the fused mass well up on the sides of the crucible and chill by dipping the bottom of the crucible in a vessel of cold water. If loose, remove the mass from...
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Portland Cement: Its Composition, Raw Materials, Manufacture, Testing and ...

Richard Kidder Meade - 1906 - 422 Seiten
...burner for a while and then over a blast lamp, until the contents of the crucible are in quiet fusion. Run the fused mass well up on the sides of the crucible and chill by dipping the bottom of the cru"cible in a vessel of cold water. If loose, remove the mass from...
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Iowa Geological Survey, Band 17

1907 - 656 Seiten
...ground clay, dried at 100° C., with 10 grams of sodium carbonate and a very little sodium nitrate. Run the fused mass well up on the sides of the crucible, allow it to cool, and treat it with hot water until thoroughly disintegrated, transferring the liquid...
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A Manual of Practical Assaying

Howard Van Fleet Furman - 1908 - 546 Seiten
...grammes of sodium nitrate. Fuse in a large platinum dish for about one hour at a high temperature. Run the fused mass well up on the sides of the crucible and allow to cool; dissolve in hot water and filter. If a 5-grammc sample was taken for analysis dilute to about...
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Portland Cement: Its Composition, Raw Materials, Manufacture, Testing and ...

Richard Kidder Meade - 1911 - 568 Seiten
...burner for a while and then over a blast lamp, until the contents of the crucible are in quiet fusion. Run the fused mass well up on the sides of the crucible and chill by dipping the bottom of the crucible in a vessel of cold water. If loose, remove the mass from...
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