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" ... permanganate used is so small as to make doubtful the presence of vanadium, it is necessary to apply a qualitative test, which is best made as follows: The solution is evaporated and heated to expel excess of sulphuric acid, the residue is taken up... "
The American Journal of Science - Seite 213
1898
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Chemical News and Journal of Industrial Science, Band 83

1901 - 392 Seiten
...to expel excess of sulphuric acid, the residue is taken up with 2 or 3 cc, of water, and a few drops of dilute nitric acid, and a couple of drops of hydrogen...sulphuric acid has been removed the appearance of this colour is sometimes not immediate and pronounced, hence the above precaution. It is also necessary...
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Chemical News and Journal of Industrial Science, Band 78

1898 - 356 Seiten
...cc of water and a drop or two of dilute nitric acid, and a couple of drops of hydrogen peroxide ate added. A characteristic brownish tint indicates vanadium....sulphuric acid has been removed the appearance of this colour is sometimes not immediate and pronounced ; hence the above precaution. The above is a surer...
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Contributions to Chemistry and Mineralogy from the Laboratory of the United ...

Frank Wigglesworth Clarke - 1900 - 984 Seiten
...solution is evaporated and heated to expel excess of sulphuric acid, the residue is taken up with 2 or 3 cubic centimeters of water and a drop or two of dilute...above is a surer test to apply than the following : tieduce the bulk to about 10 cubic centimeters, add ammonia in excess and introduce hydrogen sulphide...
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Survey of the Northwestern Boundary of the United States, 1857-1861

Marcus Baker - 1900 - 350 Seiten
...sulphuric acid, the residue is taken up with two or three cubic centimeters of water and a few drops of dilute nitric acid, and a couple of drops of hydrogen...immediate and pronounced, hence the above precaution. It is also necessary that the nitric acid shall be in considerable excess, since in a neutral or only...
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Bulletin, Ausgaben 303-308

1907 - 874 Seiten
...to expel excess of sulphuric acid, the residue is taken up with 2 or 3 cm.3 of water and a few drops of dilute nitric acid, and a couple of drops of hydrogen...immediate and pronounced, hence the above precaution. It is also necessary that the nitric acid shall be in considerable excess, since in a neutral or only...
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Technical Methods of Ore Analysis

Albert Howard Low - 1905 - 316 Seiten
...taken up with 2 or 3 cc. of water and a few drops of dilute nitric acid, and a couple of drops of H2O2 are added. A characteristic brownish tint indicates...sulphuric acid has been removed the appearance of the color is sometimes not immediate and pronounced, hence the above precaution. It is also necessary...
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Technical Methods of Ore Analysis

Albert Howard Low - 1905 - 318 Seiten
...taken up with 2 or 3 cc. of water and a few drops of dilute nitric acid, and a couple of drops of HaO2 are added. A characteristic brownish tint indicates...sulphuric acid has been removed the appearance of the color is sometimes not immediate and pronounced, hence the above precaution. It is also necessary...
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The Areas of the United States, the States, and the ..., Ausgaben 302-307

Henry Gannett - 1906 - 644 Seiten
...to expel excess of sulphuric acid, the residue is taken up with 2 or 3 cm.3 of water and a few drops of dilute nitric acid, and a couple of drops of hydrogen...sometimes not immediate and pronounced, hence the above urecaution. It is also necessary that the nitric acid shall be in considerable excess, since in a neutral...
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The Analysis of Silicate Ad Carbonate Rocks

William Francis Hillebrand - 1907 - 212 Seiten
...to expel excess of sulphuric acid, the residue is taken up with 2 or 3 cm.3 of water and a few drops of dilute nitric acid, and a couple of drops of hydrogen...immediate and pronounced, hence the above precaution. It is also necessary that the nitric acid shall be in considerable excess, since in a neutral or only...
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The Analysis of Silicate and Carbonate Rocks: A Revision of Bulletin 305

William Francis Hillebrand - 1910 - 252 Seiten
...expel excess of sulphuric acid, the residue is taken up \vith 2 or 3 cm.3 of water and a few drops of dilute nitric acid, and a couple of drops of hydrogen peroxide are added. A characteristic o From a sulphuric solution the separation of platinum and molybdenum by hydrogen sulphide is much...
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