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" ... on ignition. If an excess of acetic acid has been used, this is cautiously removed by ammonia. Then a drop or two of solution of ammonium oxalate is added, and the small beaker is set aside for twelve hours if necessary. Almost invariably a small... "
Bulletin - Seite 103
1907
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Chemical News and Journal of Industrial Science, Band 83

1901 - 392 Seiten
...hours if necessary. Almost invariably a small precipitate soon shows itself, which if fine-grained and non-adherent to the glass may be regarded as pure...re-precipitated. Its final weight, averaging perhaps one-half milligrm., is to be added to that of the lime already found, and subtracted as tricalcium phosphate...
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Chemical News and Journal of Industrial Science, Band 78

1898 - 356 Seiten
...re-solution and re-precipitation after ignition, and its weight, averaging one-half milligrm., is then added to that of the lime already found, and subtracted as tricalcium phosphate from that of the magnesium pyrophosphate, in order to arrive at the true figure for magnesium. This...
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Bulletin of the United States Geological Survey, Ausgaben 142-149

1896 - 1020 Seiten
...re-solution and reprecipitation after ignition, and its weight, averaging one-half milligram, is then added to that of the lime already found, and subtracted as tricalcium phosphate from that of the magnesium pyrophosphate, in order to arrive at the true figure for magnesium. This...
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Analyses of Rocks, with a Chapter on Analytical Methods ..., Ausgabe 147

Frank Wigglesworth Clarke, William Francis Hillebrand - 1897 - 342 Seiten
...re-solntiou and reprecipitation after ignition, and its weight, averaging one-half milligram, is then added to that of the lime already found, and subtracted as tricalcium phosphate from that of the magnesium pyrophosphate, in order to arrive at the true figure for magnesium. This...
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Survey of the Northwestern Boundary of the United States, 1857-1861

Marcus Baker - 1900 - 350 Seiten
...twelve hours if necessary. Almost invariably a small precipitate soon shows itself, which if finegrained and nonadherent to the glass may be regarded as pure...already found, and subtracted as tricalcium phosphate from that of the magnesium pyrophosphate in order to arrive at the true figure for magnesia. This separation,...
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The Areas of the United States, the States, and the ..., Ausgaben 302-307

Henry Gannett - 1906 - 644 Seiten
...quite insoluble in acids. This residue contains no silica, but only the constituents of a niagnesian phosphate, and it may be a peculiar metaphosphate....that of the magnesium pyrophosphate, in order « A pink color of varying intensity almost invariably becomes apparent as the mass approaches dryneaa,...
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Bulletin of the United States Geological Survey

Geological Survey (U.S.) - 1907 - 220 Seiten
...alkalinity, and then acetic acid, drop by drop, till the solution, which should measure 10 to 30 cm.0 and not be hot, clears. It now and then happens that...the magnesium pyrophosphate, in order a A pink color of varying intensity almost invariably becomes apparent as the mass approaches dryness, a most delicate...
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The Analysis of Silicate Ad Carbonate Rocks

William Francis Hillebrand - 1907 - 212 Seiten
...alkalinity, and then acetic acid, drop by drop, till the solution, which should measure 10 to 30 cm.o and not be hot, clears. It now and then happens that...the magnesium pyrophosphate, in order a A pink color of varying intensity almost invariably becomes apparent as the mass approaches dryness, a most delicate...
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Bulletin of the United States Geological Survey

Geological Survey (U.S.) - 1910 - 252 Seiten
...it may be filtered, ignited, and weighed as calcium oxide. Its weight, averaging less than 0.5 mg., is to be added to that of the lime already found and...from that of the magnesium pyrophosphate, in order to arrive at the true figure for magnesia. The alcoholic filtrate is to be evaporated, ignited to destroy...
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Results of Spirit Leveling in Illinois, 1896 to 1908, Inclusive

Samuel Stinson Gannett, David Henry Baldwin - 1910 - 490 Seiten
...it may be filtered, ignited, and weighed as calcium oxide. Its weight, averaging less than 0.5 mg., is to be added to that of the lime already found and...from that of the magnesium pyrophosphate, in order to arrive at the true figure for magnesia. The alcoholic filtrate is to be evaporated, ignited to destroy...
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